LIU Guang-bin,ZHANG Xun,LIU Xiao-shuan,et al.Study on Quality Standard for Shuanghuangqing Powder[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):51-53.[doi:10.3969/j.issn.1005-5304.2010.10.022]
双黄清散剂质量标准研究
- Title:
- Study on Quality Standard for Shuanghuangqing Powder
- 文章编号:
- 1005-5304(2010)10-0051-03
- Keywords:
- Shuanghuangqing Powder; HPLC; TLC; berberine hydrochloride; quality standard
- 分类号:
- R284.1
- 文献标志码:
- A
- 摘要:
- 目的 建立双黄清散剂的质量标准。方法 采用薄层色谱法鉴别人工牛黄、黄柏、青黛、甘草、龙胆草;采用高效液相色谱法测定黄柏中有效成分盐酸小檗碱的含量。结果 薄层鉴别方法专属性强,重复性好,空白无干扰;盐酸小檗碱在0.080 2~0.802 ?g范围内呈良好的线性关系,r=0.999 7,平均加样回收率为98.52%,RSD=1.05%(n=9)。结论 本研究中建立的定性定量方法操作简便,专属性强,准确可靠,可以有效控制双黄清散剂的质量。
- Abstract:
- Objective To establish the quality standard of Shuanghuangqing Powder. Methods Artificial Calculus Bovis, Cortex Phellodendri Chinensis, Indigo Naturalis, Radix Glycyrrhizae, Radix Gentianae in Shuanghuangqing Powder were identified by TLC, and content of berberine hydrochloride was determined by HPLC. Results The method for identification had good specificity and repeatability. There was no interference in blank control. The berberine hydrochloride determination method had good linearity from 0.080 2 to 0.802 ?g (r=0.999 7). The average recovery was 98.52% and the relative standard deviation (RSD) was 1.05% (n=9). Conclusion The qualitative and quantitative method is simple, specific, accurate and reliable. It can be used to effectively control the quality of Shuanghuangqing Powder.
参考文献/References:
[1] 国家药典委员会.中华人民共和国药典(一部)[S].北京:化学工业出版社,2005.48,214,138,59,64,99,236.
相似文献/References:
[1]蔡俊安.高效液相色谱法测定二妙丸中盐酸小檗碱的含量[J].中国中医药信息杂志,2011,18(1):55.[doi:10.3969/j.issn.1005-5304.2011.01.022]
CAI Jun-an.Determination of Berberine Hydrochloride in Ermiao Wan by HPLC[J].zhongguo zhongyiyao xinxi zazhi,2011,18(10):55.[doi:10.3969/j.issn.1005-5304.2011.01.022]
[2]费超,孟蕾,张海鸣,等.高效液相色谱法测定虫草安肺片中盐酸麻黄碱含量[J].中国中医药信息杂志,2011,18(1):57.[doi:10.3969/j.issn.1005-5304.2011.01.023]
FEI Chao,MENG Lei,ZHANG Hai-ming,et al.Determination of Ephedrine Hydrochloride in Chongcaoanfei Tablets by HPLC[J].zhongguo zhongyiyao xinxi zazhi,2011,18(10):57.[doi:10.3969/j.issn.1005-5304.2011.01.023]
[3]仵树仁,蔡俊安,郭鑫慧.感特灵胶囊中黄芩苷的HPLC测定[J].中国中医药信息杂志,2010,17(5):49.
WU Shu-ren,CAI Jun-an,GUO Xin-hui.Determination of Baicalin in Ganteling Jiaonang by HPLC[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):49.
[4]宋平顺,杨树声,马真金,等.酒制甘肃丹参的炮制工艺研究[J].中国中医药信息杂志,2010,17(5):51.
SONG Ping-shun,YANG Shu-sheng,MA Zhen-jin,et al.Study on Processing Technology of Wine Gansu Salvia[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):51.
[5]刘宏明,赵昌军.高效液相色谱法测定六味五灵片中连翘苷的含量[J].中国中医药信息杂志,2010,17(11):48.
[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):48.
[6]李 慧,方清影,王艳荣,等.高效液相色谱法测定纳米给药系统斑蝥素囊泡中药物的含量和包封率[J].中国中医药信息杂志,2010,17(12):39.[doi:10.3969/j.issn.1005-5304.2010.12.016]
LI Hui,FANG Qing-ying,WANG Yan-rong,et al.Determination of Entrapment Efficiency and the Contents of Cantharidin Niosome by HPLC[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):39.[doi:10.3969/j.issn.1005-5304.2010.12.016]
[7]闫 艳,张淑蓉,裴香萍,等.山西道地连翘HPLC-UV指纹图谱研究[J].中国中医药信息杂志,2010,17(12):41.[doi:10.3969/j.issn.1005-5304.2010.12.017]
YAN Yan,ZHANG Shu-rong,PEI Xiang-ping,et al.Study on Fingerprints of Fructus Forsythiae from Shanxi Province by HPLC-UV[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):41.[doi:10.3969/j.issn.1005-5304.2010.12.017]
[8]原红霞,裴妙荣,裴香萍,等.高效液相色谱法测定健脾养胃胶囊中黄芩苷的含量[J].中国中医药信息杂志,2010,17(12):52.[doi:10.3969/j.issn.1005-5304.2010.12.022]
YUAN Hong-xia,Pei Miao-rong,Pei Xiang-ping,et al.Determination of Baicalin in Jianpi-yangwei Capsules by High Performance Liquid Chromatogrphy[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):52.[doi:10.3969/j.issn.1005-5304.2010.12.022]
[9]彭晓霞,张振巍,迟栋,等.两种不同提取方法对赤芍中丹皮酚含量的影响[J].中国中医药信息杂志,2010,17(2):46.
PENG Xiao-xia,ZHANG Zhen-wei,CHI Dong,et al.Effect of Two Extracting Methods on Content of Paeonol in Paeonia lactiflora Pall. by HPLC[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):46.
[10]古海锋,刘然,张小茜,等.安神健脑液质量标准研究[J].中国中医药信息杂志,2010,17(2):50.
GU Hai-feng,LIU Ran,ZHANG Xiao-qian,et al.Study on the Quality Standard of Anshen Jiannao Mixture[J].zhongguo zhongyiyao xinxi zazhi,2010,17(10):50.
更新日期/Last Update: